Effect of Different Photoiniciers of Experimental Adhesive Systems on Adhesive Interface Union Resistance
Abstract
Aim: The objective of this study was to investigate the performance of experimental resinous adhesives containing different combinations of photoinitiators systems through the bending test.
Material and Methods: Resinous adhesive formulations were prepared with monomer mixtures consisting of 50% by mass of bisphenol dimethacrylate glycidyl (BisGMA) and 50% by mass of triethyleneglycol dimethacrylate (TEGDMA). The photoinitiators were used, camphorquinone (CQ) and bis-alkyl phosphinic oxide (BAPO). The co-initiators were diphenyliodonium hexafluorophosphate (DFI) and the amine (dimethylamino methylmethacrylate - DMAEMA) in the 1:1 proportion by mass. The photopolymerizable initiator systems were dissolved in the organic matrix at 0.5% by mass concentrations, creating eight groups (G1- CQ, G2- CQ/amine, G3- CQ/DFI, G4- CQ/amine/DFI, G5- BAPO, G6- BAPO/amine, G7- BAPO/DFI, G8- BAPO/amine/DFI). Samples with 7.0 mm in length, 2.0 mm wide and 1.0 mm height were prepared (n=12). The curing light used was VALO – Ultradent and the curing time was 20 s. The samples were subjected to evaluation of bending test at three points at a speed of 1 mm/min to evaluate the flexural resistance (FR).
Results: The results were submitted to analysis of variance with one criterion (p < 0,001) and multiple comparisons were performed using Tukey test. Systems with the photoinitiator BAPO showed higher or equivalent bending values that demonstrated by the conventional system containing CQ/amine. Systems with the DFI had higher flexural values in relation to those demonstrated by systems without the DFI to CQ.
Conclusion: The use of systems with alternative photoinitiators and co-initiators allows to obtain superior properties to the conventional system, making these promising systems to act both in isolation as associated with conventional systems.
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20. Christensen T, Morisbak E, Tonnesen HH, Bruzell EM. In vitro photosensitization initiated by camphoquinone and phenyl propanedione in dental polymeric materials. J Photoch Photobio B: Biology. 2010;100:128-34.
21. Cook WD. Photopolymerization kinetics of dimethacrylates usin the canforquinona/amine initiator system. Polymer. 1992;33(3):600-9.
22. Corrales T, Catalina F, Peinado C, Allen NS. Journal of photochemistry and photobiology A. Chemistry.2003;159:103.
23. Correa IC. Análise do grau de conversão de uma resina experimental fotopolimerizável: um estudo espectrofotométrico em função de diferentes fotoiniciadores e fontes de luz [tese]. São Paulo: Universidade de São Paulo; 2003.
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25. Decker C, Zahouily K, Decker D, Nguyen T, Viet THI. Performance analysis of acylphosphine oxides in photoinitiated polymerization. Polymer. 2001;42(18):7551-60.
26. Dewaele M, Asmussen E, Peutzfeldt A, Munksgaard EC, Benetti AR, Finné G, et al. Influence of curing protocol on selected properties of light-curing polymers: degree of conversion, volumer contraction, elastic modulus and glass transition temperature. Dent Mater. 2009;25:1576-84.
27. Ely C, Schneider LF, Ogliari FA, Schmitt CC, Correa IC, LimaGS, et al. Polymerization kinetics and reactivity of alternative initiators systems for use in light-activated dental resins. Dent Mater. 2012;28(12):1199–206.
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31. Garcia RN, Souza CRS, Mazucco PEF, Justino, LM, Schein MT, Giannini M. Avaliação da resistência de união de dois sistemas adesivos autocondicionantes – Revisão de literatura e aplicação do ensaio de microcisalhamento. RSBO. 2007; 4 (1):37-44.
32. Gonçalves LS, Moraes RR, Ogliari FA, Boaro L, Braga, RR, Consani S. Improved polymerization efficiency of methacrylate-based cements containing an iodonium salt. Dental Mater.2013; 22-56.
33. Gonçalves,J, Castanho GM, kimpara ET, Uemura ES, Alberto Cara A. Current adhesive systems and perspectives. Revista Odonto • Ano 16, n. 31, jan. jun. 2008, São Bernardo do Campo, SP, Metodista.
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35. Ikemura K, Endo T. A review of the development of radical photopolymerization initiators used for designing light-curing dental adhesives and resin composites. Dent Mater J. 2010 Oct;29(5):481-501.
36. Ikemura K, Ichizawa K, Jogetsu Y, Endo T. Synthesis of a novel camphorquinone derivative having acylphosphine oxide group, characterization by UV-Vis espectroscopy and evaluation of photopolimerization performance. Dent Mater J. 2010;29(2):122-31.
37. Ikemura K, Ichizawa K, Yoshida M, Ito S, Endo T. UV-VIS spectra and photoinitiation behaviors of acylphosphine oxide and bisacylphosphine oxide derivatives in unfilled, light-cured dental resins. Dent Mater J. 2008;27(6):765-74.
38. Ilie N, Hickel R. Can CQ be completely replaced by alternative initiators in dental adhesives? Dent Mater J. 2008;27(2):221-8.
39. Ilie N, Hickel R. Resin composite restorative materials. Aust Dent J. 2011;56(1):59- 66.
40. Jakubiak J, Allonas X, Fouassier JP, Sionkowska A, Andrzejewska E, Linden LA, Rabek JF. Camphorquinone – amines photoinitating systems for the initiation of free radical polymerization. Polymer. 2003;44:5219-26.
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Published
2018-05-12
How to Cite
GOMES, Tiago Norões et al.
Effect of Different Photoiniciers of Experimental Adhesive Systems on Adhesive Interface Union Resistance.
International Archives of Medicine, [S.l.], v. 11, may 2018.
ISSN 1755-7682.
Available at: <http://imedicalpublisher.com/ojs/index.php/iam/article/view/2813>. Date accessed: 01 june 2023.
doi: https://doi.org/10.3823/2567.
Issue
Section
Dental Medicine
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